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Phase Structure of Block and Gradient Copolymers of Butyl Acrylate and Styrene

Published on Mar 1, 2020in Polymer Science Series A0.984
· DOI :10.1134/S0965545X20010010
A. E. Chalykh8
Estimated H-index: 8
,
U. V. Nikulova1
Estimated H-index: 1
+ 1 AuthorsR. R. Khasbiullin3
Estimated H-index: 3
Abstract
  • References (6)
  • Citations (0)
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#1A. E. Chalykh (RAS: Russian Academy of Sciences)H-Index: 8
#2V. K. Gerasimov (RAS: Russian Academy of Sciences)H-Index: 3
Last. I. A. GritskovaH-Index: 3
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The structures of individual polystyrene microspheres obtained in the presence of organosilicon surfactants were studied by transmission electron microscopy. The density of the macro-molecule distribution over the cross section of particles was determined. The synthesized latex particles have a core—shell structure.
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#1A. E. Chalykh (RAS: Russian Academy of Sciences)H-Index: 7
#2U. V. Nikulova (RAS: Russian Academy of Sciences)H-Index: 2
Last. A. A. Shcherbina (RAS: Russian Academy of Sciences)H-Index: 4
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Phase equilibria in polystyrene-poly(n-butyl acrylate) systems containing polystyrene of various molecular masses were studied for the first time via optical interferometry at temperatures between 280 and 500 K. The phase diagrams of the systems were obtained, the pair interaction parameters were determined, and the dependences of the parameters on the molecular mass of polystyrene and temperature were found. The possibility of thermodynamic analysis of phase diagrams in terms of the classical F...
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#1Elena Chernikova (MSU: Moscow State University)H-Index: 12
#2V. V. Yulusov (MSU: Moscow State University)H-Index: 5
Last. A. Yu. Nikolaev (MSU: Moscow State University)H-Index: 9
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Copolymers of styrene and n-butyl acrylate are synthesized via pseudoliving radical copolymerization mediated by dibenzyl trithiocarbonate as a reversible addition fragmentation chain transfer agent. In a wide range of monomer feed compositions, narrowly dispersed compositionally uniform copolymers of desired molecular masses are formed, and their gradient structures are controlled by the compositions of the initial monomer feeds. The effects of the compositions, the chain microstructures, and t...
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1 Introduction.- 2 Types of Differential Scanning Calorimeters and Modes of Operation.- 3 Theoretical Fundamentals of Differential Scanning Calorimeters.- 4 Calibration of Differential Scanning Calorimeters.- 5 DSC Curves and Further Evaluation.- 6 Applications of Differential Scanning Calorimetry.- 7 Evaluation of the Performance of a Differential Scanning Calorimeter.- Appendix 1.- Appendix 2.- References.
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