On the synthesis and structure of the copper-molybdenum oxide bronzes: Monoclinic Cu2Mo10O30 and orthorhombic CuMo9O26
Abstract
Cu2Mo10O30 was prepared as a monophasic material comprising dark blue platy crystals by reacting Cu with MoO3 under argon at 550 °C. Single-crystal X-ray diffractometry showed that Cu2Mo10O30 is a stoichiometric compound that crystallizes with a monoclinic (C2/c) cell: a = 16.6359(6); b = 9.3112(3); c = 27.1597(9) Å; β = 102.621(3)° (Z = 8). Electron paramagnetic resonance spectroscopy revealed that Cu2Mo10O30 displays mixed-valency;...
Paper Details
Title
On the synthesis and structure of the copper-molybdenum oxide bronzes: Monoclinic Cu2Mo10O30 and orthorhombic CuMo9O26
Published Date
May 1, 2020
Volume
285
Pages
121259 - 121259
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