Original paper
Synthesis of Karrikinolide Using the Aldol-Type Acetal Addition Reaction
Abstract
A short step total synthesis of karrikinolide has been achieved. Both α and α′ positions of O-acylated acetol were alkylated by the boron-mediated aldol-type acetal addition reaction. The one-pot sequence including the Arbuzov reaction, intramolecular Horner–Wadsworth–Emmons reaction, acidic hydrolysis of acetals, and pyran formation provided karrikinolide. This procedure was applicable to the gram-scale synthesis of...
Paper Details
Title
Synthesis of Karrikinolide Using the Aldol-Type Acetal Addition Reaction
Published Date
Jan 24, 2020
Volume
85
Issue
5
Pages
3936 - 3941
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