Ni(II)/Al(0) mediated benzylic $$\hbox {Csp}^{3}$$-$$\hbox {Csp}^{3}$$ coupling in aqueous media
Abstract
The reaction of benzyl bromides and chlorides with aluminium metal powder or foil (1.2 eqv.) in the presence of catalytic nickel nitrate (10 mol%) in water at room temperature resulted in homocoupling to the corresponding bibenzyl products which were isolated in moderate to good yields. In sharp contrast, the same reaction in organic solvents like dichloromethane, dimethylformamide, acetonitrile, methanol and toluene yielded only a trace amount...
Paper Details
Title
Ni(II)/Al(0) mediated benzylic $$\hbox {Csp}^{3}$$-$$\hbox {Csp}^{3}$$ coupling in aqueous media
Published Date
Jul 1, 2019
Journal
Volume
131
Issue
7
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