Sodium sulfide in methanol: a two-in-one reagent for deprotection of silyl and formation of propargyl sulfide
Abstract
A new reagent Na2S/MeOH for silyl deprotection has been developed. The reagent has several advantages which include deprotection of C-TMS, O-TMS, O-TBS, and O-TBDPS, selective removal of C-TMS and O-TMS in the presence of O-TBS and simultaneous desilylation and sulfide formation in one...
Paper Details
Title
Sodium sulfide in methanol: a two-in-one reagent for deprotection of silyl and formation of propargyl sulfide
Published Date
May 14, 2015
Journal
Volume
56
Issue
29
Pages
4275 - 4279
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