Integrating31P DOSY NMR Spectroscopy and Molecular Mechanics as a Powerful Tool for Unraveling the Chemical Structures of Polyoxomolybdate-Based Amphiphilic Nanohybrids in Aqueous Solution
Abstract
Novel organic–inorganic hybrids of various sizes were generated by reaction of 1,8‐octanediphosphonic acid (ODP) and (NH 4 ) 6 Mo 7 O 24 in aqueous solution. The formation of rodlike hybrids with variable numbers of covalently bound ODP and polyoxomolybdate (POM) units can be tuned as a function of increasing (NH 4 ) 6 Mo 7 O 24 concentration at fixed ODP concentration. The chemical structure of the ODP/POM hybrids was characterized by 1 H, 31...
Paper Details
Title
Integrating31P DOSY NMR Spectroscopy and Molecular Mechanics as a Powerful Tool for Unraveling the Chemical Structures of Polyoxomolybdate-Based Amphiphilic Nanohybrids in Aqueous Solution
Published Date
Apr 11, 2014
Volume
20
Issue
18
Pages
5258 - 5270
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