Modeling in Organotin Chemistry Using NMR Restraints: A Case Study on the 9R,12S-[tBu2Sn]2O Derivative of Erythromycin A

Volume: 121, Issue: 14, Pages: 3284 - 3291
Published: Mar 23, 1999
Abstract
The 9R,12S-[tBu2Sn]2O derivative of the macrolide antibiotic erythromycin A (ErySn-A) is obtained as the sole regio- and stereospecific reaction product from the condensation reaction of (tBu2SnOPr)2O with erythromycin A in benzene solution. Complete resonance assignments were achieved, and the covalent structure was derived using various one-dimensional and two-dimensional NMR techniques, including gradient enhanced 1H−119Sn heteronuclear...
Paper Details
Title
Modeling in Organotin Chemistry Using NMR Restraints: A Case Study on the 9R,12S-[tBu2Sn]2O Derivative of Erythromycin A
Published Date
Mar 23, 1999
Volume
121
Issue
14
Pages
3284 - 3291
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